C₃₁H₃₉FN₄O₄

Base Information

Chemical Name:C₃₁H₃₉FN₄O₄
CAS No.:1047666-82-9
Molecular Formula:C₃₁H₃₉FN₄O₄
Molecular Weight:550.673
Hs Code.:

C<sub>31</sub>H<sub>39</sub>FN<sub>4</sub>O<sub>4</sub>

Synonyms:C₃₁H₃₉FN₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₃₉FN₄O₄

Chemical Property:

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Technology Process of C₃₁H₃₉FN₄O₄

There total 20 articles about C₃₁H₃₉FN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49606-99-7,5687-71-8,15785-26-9,49607-01-4
(S)-2-amino-2-cyclopropylacetic acid

: 1047666-82-9
C₃₁H₃₉FN₄O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / 20 °C / Inert atmosphere

2.1: pyridine; triethylamine / dichloromethane / 20 °C / Inert atmosphere

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

4.1: propylamine; 3-mercaptopropionic acid / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

5.1: N,N-diethyl-N-isopropylamine; HATU / tetrahydrofuran; dichloromethane / 20 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / Inert atmosphere

6.2: 20 °C / Inert atmosphere

7.1: N,N-diethyl-N-isopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 20 °C / Inert atmosphere

With pyridine; propylamine; N,N-diethyl-N-isopropylamine; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; HATU; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; 3-mercaptopropionic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm2007062

Reference yield:

: 18125-46-7
(R)-4-fluorophenylalanine

: 1047666-82-9
C₃₁H₃₉FN₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: Inert atmosphere; Reflux

2.1: N,N-diethyl-N-isopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 6-chloro-1-hydroxybenzotriazole / tetrahydrofuran; dichloromethane / 20 °C / Inert atmosphere

3.1: hydrogenchloride / ethyl acetate / 20 °C / Inert atmosphere

4.1: N,N-diethyl-N-isopropylamine; HATU / tetrahydrofuran; dichloromethane / 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / Inert atmosphere

5.2: 20 °C / Inert atmosphere

6.1: N,N-diethyl-N-isopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 20 °C / Inert atmosphere

With hydrogenchloride; N,N-diethyl-N-isopropylamine; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 6-chloro-1-hydroxybenzotriazole; HATU; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm2007062

Reference yield:

: C₃₁H₄₁FN₄O₅

: 1047666-82-9
C₃₁H₃₉FN₄O₄

Guidance literature:: With N,N-diethyl-N-isopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm2007062