C₁₈H₂₄Cl₂NO₁₅P₃

Base Information

Chemical Name:C₁₈H₂₄Cl₂NO₁₅P₃
CAS No.:1351399-98-8
Molecular Formula:C₁₈H₂₄Cl₂NO₁₅P₃
Molecular Weight:658.214
Hs Code.:

C<sub>18</sub>H<sub>24</sub>Cl<sub>2</sub>NO<sub>15</sub>P<sub>3</sub>

Synonyms:C₁₈H₂₄Cl₂NO₁₅P₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₄Cl₂NO₁₅P₃

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Technology Process of C₁₈H₂₄Cl₂NO₁₅P₃

There total 2 articles about C₁₈H₂₄Cl₂NO₁₅P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1351399-95-5
C₁₃H₁₇IO₅

: 1351399-98-8
C₁₈H₂₄Cl₂NO₁₅P₃

Guidance literature:: C₁₃H₁₇IO₅; With trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate; at -15 - -10 ℃; for 2h; Inert atmosphere;

With tributyl-amine; bis(tri-n-butylammonium) pyrophosphate; In N,N-dimethyl-formamide; at -10 - 0 ℃; Inert atmosphere;

With triethylamine carbonate; In water; N,N-dimethyl-formamide; at 0 ℃; pH=7.5;
DOI:10.1021/ja207907d

Reference yield:

: 1135561-91-9
C₁₃H₁₈O₅

: 1351399-98-8
C₁₈H₂₄Cl₂NO₁₅P₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; silver nitrate / methanol / 20 °C

2.1: trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / 2 h / -15 - -10 °C / Inert atmosphere

2.2: -10 - 0 °C / Inert atmosphere

2.3: 0 °C / pH 7.5

With trimethyl phosphite; iodine; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; silver nitrate; trichlorophosphate; In methanol;
DOI:10.1021/ja207907d