meso-phenylpentanedioic acid

Base Information

Chemical Name:meso-phenylpentanedioic acid
CAS No.:220271-74-9
Molecular Formula:C₁₉H₂₀O₄
Molecular Weight:312.365
Hs Code.:

Synonyms:meso-phenylpentanedioic acid

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Chemical Property of meso-phenylpentanedioic acid

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Technology Process of meso-phenylpentanedioic acid

There total 4 articles about meso-phenylpentanedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 220271-72-7
meso-phenylpentanedinitrile

: 220271-74-9
meso-phenylpentanedioic acid

Guidance literature:: With potassium hydroxide; In ethanol; water; at 80 ℃; for 18h;
DOI:10.1016/S0040-4039(98)02179-0

Reference yield:

: 2947-61-7
(4-methylphenyl)acetonitrile

: 220271-74-9
meso-phenylpentanedioic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 8.1 g / NaOH / 0.75 h / 165 °C

2: 6.2 g / KOH / ethanol; H₂O / 18 h / 80 °C

With potassium hydroxide; sodium hydroxide; In ethanol; water; 1: Substitution / 2: Hydrolysis;
DOI:10.1021/jo991741p

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 220271-74-9
meso-phenylpentanedioic acid

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 4 h / 20 °C

2: potassium carbonate / 1,4-dioxane / 6 h / 110 °C / Inert atmosphere; Schlenk technique

3: tetrabutylammonium tetrafluoroborate / 1-methyl-pyrrolidin-2-one / 12 h / 20 °C / 760.05 Torr / Electrochemical reaction

With tetrabutylammonium tetrafluoroborate; potassium carbonate; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol;
DOI:10.1021/jacs.1c12071