1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester

Base Information

Chemical Name:1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester
CAS No.:835925-54-7
Molecular Formula:C₃₃H₅₁NO₆S
Molecular Weight:589.837
Hs Code.:

1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid <i>tert</i>-butyl ester

Synonyms:1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester

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Chemical Property of 1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester

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Technology Process of 1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester

There total 6 articles about 1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 738606-92-3
t-butyl 1-(5-iodopentyl)-1-cyclopropanecarboxylate

: 738607-02-8
{8-Ethoxy-7,7-dimethyl-1-[(4-methylphenyl)sulfonyl]-8-oxooctyl}(methylidene)ammonium

: 835925-54-7
1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl acetamide; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2004.09.046

Reference yield:

: 738606-91-2
t-butyl 1-(5-chloropentyl)-1-cyclopropanecarboxylate

: 835925-54-7
1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / NaI / butan-2-one / Heating

2: 43.02 g / KOtBu / N,N-dimethyl-acetamide / 0 - 20 °C

With potassium tert-butylate; sodium iodide; In N,N-dimethyl acetamide; butanone;
DOI:10.1016/j.bmc.2004.09.046

Reference yield:

: 54512-75-3
1-bromo-5-chloropentane

: 835925-54-7
1-[12-ethoxycarbonyl-6-isocyano-12-methyl-6-(toluene-4-sulfonyl)-tridecyl]-cyclopropanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropylamide / tetrahydrofuran; hexane / -70 - -35 °C

1.2: 73 percent / tetrahydrofuran; hexane / 3 h / -5 °C

2.1: 99 percent / NaI / butan-2-one / Heating

3.1: 43.02 g / KOtBu / N,N-dimethyl-acetamide / 0 - 20 °C

With potassium tert-butylate; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; hexane; N,N-dimethyl acetamide; butanone;
DOI:10.1016/j.bmc.2004.09.046