2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione

Base Information

Chemical Name:2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione
CAS No.:1293912-48-7
Molecular Formula:C₃₁H₂₅NO₇S
Molecular Weight:555.608
Hs Code.:

Synonyms:2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione

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Chemical Property of 2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione

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Technology Process of 2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione

There total 10 articles about 2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1293912-50-1
4-(1,3-dioxo-1,3-dihydrobenzo[f]isoindol-2-yl)benzaldehyde

: 2936-70-1,5624-48-6,13992-15-9,16758-34-2,28244-97-5,77481-62-0,77481-63-1,105088-17-3,149495-84-1
(2R,3S,4S,5R,6S)-2-Hydroxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3,4,5-triol

: 1293912-48-7
2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione

Guidance literature:: With p-toluenesulfonic acid monohydrate; In N,N-dimethyl-formamide; benzene; for 4h; under 17 Torr; Reflux; Dean-Stark apparatus;
DOI:10.1016/j.tetlet.2011.01.149

Reference yield: 40.0%

: C₁₉H₁₁Br₂NO₂

: 2936-70-1,5624-48-6,13992-15-9,16758-34-2,28244-97-5,77481-62-0,77481-63-1,105088-17-3,149495-84-1
(2R,3S,4S,5R,6S)-2-Hydroxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3,4,5-triol

: 1293912-48-7
2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione

Guidance literature:: With pyridine;
DOI:10.1016/j.tetlet.2011.01.149

Reference yield:

: D-glucose

: 1293912-48-7
2-[4-(7,8-dihydroxy-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-2-yl)-phenyl]-benzo[f]isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine

2: boron trifluoride diethyl etherate / dichloromethane

3: methanol; sodium methylate

4: pyridine

With pyridine; methanol; boron trifluoride diethyl etherate; sodium methylate; In dichloromethane;
DOI:10.1016/j.tetlet.2011.01.149