N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide

Base Information

Chemical Name:N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide
CAS No.:1321626-02-1
Molecular Formula:C₁₅H₁₃N₃O₃S
Molecular Weight:315.353
Hs Code.:

Synonyms:N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide

Chemical Property:

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Technology Process of N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide

There total 6 articles about N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈H₅ClN₂O₃S

: 100-61-8
N-methylaniline

: 1321626-02-1
N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 0.5h;
DOI:10.1002/cmdc.201200386

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 1321626-02-1
N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide

Guidance literature:: Multi-step reaction with 6 steps

1.1: nitromethane / 0.5 h / -40 °C

1.2: 1 h / 110 °C

2.1: sodium hydroxide; potassium permanganate / water / 7 h / 0 - 80 °C

2.2: pH 1

3.1: sulfuric acid / water / 6 h / 140 °C

3.2: 0.5 h / 0 °C

4.1: 2 h / Reflux

5.1: thionyl chloride / 75 °C

6.1: triethylamine / acetonitrile / 0.5 h / 20 °C

With potassium permanganate; thionyl chloride; sulfuric acid; triethylamine; sodium hydroxide; In nitromethane; water; acetonitrile;
DOI:10.1002/cmdc.201200386

Reference yield:

: 201224-76-2
3-oxo-3,4-dihydro-2H-benzo[e][1,2,4]thiadiazine-7-carboxylic acid 1,1-dioxide

: 1321626-02-1
N-methyl-N-phenyl-4H-benzo[e][1,2,4]thiadiazine-7-carboxamide-1,1-dioxide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / water / 6 h / 140 °C

1.2: 0.5 h / 0 °C

2.1: 2 h / Reflux

3.1: thionyl chloride / 75 °C

4.1: triethylamine / acetonitrile / 0.5 h / 20 °C

With thionyl chloride; sulfuric acid; triethylamine; In water; acetonitrile;
DOI:10.1002/cmdc.201200386