2-((E)-buta-1,3-dienyl)phenyl 2E-butenoate

Base Information

Chemical Name:2-((E)-buta-1,3-dienyl)phenyl 2E-butenoate
CAS No.:475490-25-6
Molecular Formula:C₁₄H₁₄O₂
Molecular Weight:214.264
Hs Code.:

Synonyms:2-((E)-buta-1,3-dienyl)phenyl 2E-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((E)-buta-1,3-dienyl)phenyl 2E-butenoate

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Technology Process of 2-((E)-buta-1,3-dienyl)phenyl 2E-butenoate

There total 2 articles about 2-((E)-buta-1,3-dienyl)phenyl 2E-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 625-35-4,3488-22-0,10487-71-5
trans-chrotonyl chloride

: 22573-29-1
(E)-1-(2-hydroxyphenyl)butadiene

: 475490-25-6
2-((E)-buta-1,3-dienyl)phenyl 2E-butenoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jo0607818

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 475490-25-6
2-((E)-buta-1,3-dienyl)phenyl 2E-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / n-BuLi / tetrahydrofuran; hexane / 4 h / -18 - 20 °C

2: 75 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂ / 0.5 h / 20 °C

With dmap; n-butyllithium; triethylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/jo0607818