benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate

Base Information

Chemical Name:benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate
CAS No.:1316231-13-6
Molecular Formula:C₅₀H₅₂NO₉P
Molecular Weight:841.938
Hs Code.:

Synonyms:benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate

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Chemical Property of benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate

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Technology Process of benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate

There total 4 articles about benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₀H₅₂NO₈P

: 1316231-13-6
benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/ja203574u

Reference yield:

: 1316231-06-7
benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-((benzyloxy)methyl)cyclohexyl)carbamate

: 1316231-13-6
benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; zinc(II) chloride / 5 h / 20 °C / Inert atmosphere

2: sodium methylate / methanol / 0 - 20 °C / Inert atmosphere

3: 1H-tetrazole / dichloromethane / 1 h / 20 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

With 1H-tetrazole; sodium methylate; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc(II) chloride; In methanol; dichloromethane;
DOI:10.1021/ja203574u

Reference yield:

: 1316231-10-3
((1R,2R,3S,4S,5S)-2,3,4-tris(benzyloxy)-5-(((benzyloxy)carbonyl)amino)cyclohexyl)methyl acetate

: 1316231-13-6
benzyl ((1S,2S,3S,4R,5R)-2,3,4-tris(benzyloxy)-5-(((bis(benzyloxy)phosphoryl)oxy)methyl)cyclohexyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 0 - 20 °C / Inert atmosphere

2: 1H-tetrazole / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

With 1H-tetrazole; sodium methylate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1021/ja203574u