methyl 3-[1-N-(benzyloxycarbonylamino)-3-phenylpropyl]hydroxyphosphinylpropanoate

Base Information

Chemical Name:methyl 3-[1-N-(benzyloxycarbonylamino)-3-phenylpropyl]hydroxyphosphinylpropanoate
CAS No.:725707-40-4
Molecular Formula:C₂₁H₂₆NO₆P
Molecular Weight:419.414
Hs Code.:

Synonyms:methyl 3-[1-N-(benzyloxycarbonylamino)-3-phenylpropyl]hydroxyphosphinylpropanoate

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Chemical Property of methyl 3-[1-N-(benzyloxycarbonylamino)-3-phenylpropyl]hydroxyphosphinylpropanoate

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Technology Process of methyl 3-[1-N-(benzyloxycarbonylamino)-3-phenylpropyl]hydroxyphosphinylpropanoate

There total 2 articles about methyl 3-[1-N-(benzyloxycarbonylamino)-3-phenylpropyl]hydroxyphosphinylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 234452-57-4
(1-{[(benzyloxy)carbonyl]amino}-3-phenylpropyl)phosphinic acid

: 725707-40-4
methyl 3-[1-N-(benzyloxycarbonylamino)-3-phenylpropyl]hydroxyphosphinylpropanoate

Guidance literature:: (1-{[(benzyloxy)carbonyl]amino}-3-phenylpropyl)phosphinic acid; With 1,1,1,3,3,3-hexamethyl-disilazane; at 110 ℃;

acrylic acid methyl ester; at 90 ℃;
DOI:10.3390/ijms22105090

Reference yield:

: 125402-54-2
(R,S)-((1-amino)-3-phenylpropyl) phosphinic acid

: 725707-40-4
methyl 3-[1-N-(benzyloxycarbonylamino)-3-phenylpropyl]hydroxyphosphinylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water

2.1: 1,1,1,3,3,3-hexamethyl-disilazane / 110 °C

2.2: 90 °C

With 1,1,1,3,3,3-hexamethyl-disilazane; In water; 2.1: |Michael Addition / 2.2: |Michael Addition;
DOI:10.3390/ijms22105090