ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate

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Chemical Name:ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate
CAS No.:304678-76-0
Molecular Formula:C₂₆H₂₂N₆O₂
Molecular Weight:450.5
Hs Code.:

Synonyms:ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate

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Chemical Property of ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate

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Technology Process of ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate

There total 4 articles about ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 304678-70-4
ethyl 5-(3-aminophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate

: 304678-76-0
ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate

Guidance literature:: ethyl 5-(3-aminophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate; With sodium nitrite; In water; acetic acid; at 0 - 5 ℃; for 1h;

With sodium azide; In water; acetic acid; at 20 ℃; for 24h;
DOI:10.3987/com-00-8960

Reference yield:

: 61404-76-0
2-amino-3-cyano-4-methyl-5-phenylpyrrole

: 304678-76-0
ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 94 percent / acetic acid / 6 h / Heating

2.1: 90 percent / H₂ / 10 percent Pd-C / ethanol / 20 °C / 2585.74 Torr

3.1: NaNO₂ / acetic acid; H₂O / 1 h / 0 - 5 °C

3.2: 86 percent / NaN₃ / acetic acid; H₂O / 24 h / 20 °C

With hydrogen; sodium nitrite; palladium on activated charcoal; In ethanol; water; acetic acid;
DOI:10.3987/com-00-8960

Reference yield:

: 118209-48-6
ethyl 1-(3-nitrophenyl)-1,4-pentanedione-3-carboxylate

: 304678-76-0
ethyl 5-(3-azidophenyl)-1-(3-cyano-4-methyl-5-phenylpyrrol-2-yl)-2-methylpyrrole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 94 percent / acetic acid / 6 h / Heating

2.1: 90 percent / H₂ / 10 percent Pd-C / ethanol / 20 °C / 2585.74 Torr

3.1: NaNO₂ / acetic acid; H₂O / 1 h / 0 - 5 °C

3.2: 86 percent / NaN₃ / acetic acid; H₂O / 24 h / 20 °C

With hydrogen; sodium nitrite; palladium on activated charcoal; In ethanol; water; acetic acid;
DOI:10.3987/com-00-8960