Mn(C₅H₄CH₃)(CH₂CHCH₂Si(C₆H₅)3)(CO)2

Base Information

• Chemical Name: Mn(C₅H₄CH₃)(CH₂CHCH₂Si(C₆H₅)3)(CO)2
• CAS No.: 89958-53-2
• Molecular Formula: C₂₉H₂₇MnO₂Si
• Molecular Weight: 490.556

Synonyms:Mn(C₅H₄CH₃)(CH₂CHCH₂Si(C₆H₅)3)(CO)2

Chemical Property of Mn(C₅H₄CH₃)(CH₂CHCH₂Si(C₆H₅)3)(CO)2

Chemical Property:

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Technology Process of Mn(C₅H₄CH₃)(CH₂CHCH₂Si(C₆H₅)3)(CO)2

There total 1 articles about Mn(C₅H₄CH₃)(CH₂CHCH₂Si(C₆H₅)3)(CO)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

methylcyclopentadienyl manganese(I) tricarbonyl + allyltriphenylsilane (18752-21-1) → Mn(C5H4CH3)(CH2CHCH2Si(C6H5)3)(CO)2 (89958-53-2)

Guidance literature:

In tetrahydrofuran; Irradiation (UV/VIS); A soln. of reagents in THF was irradiated with a 100-W Hanovia lamp overnight (N2 atm.);; solvent was pumped off, ppt. was crystd. from hexane at -20°C;;

Reference yield: 70.0%

Mn(C5H4CH3)(CH2CHCH2Si(C6H5)3)(CO)2 (89958-53-2) → (methylcyclopentadienyl)Mn(CO)2PPh3 + allyltriphenylsilane (18752-21-1)

Guidance literature:

With triphenylphosphine; In toluene; A soln. of reagents in toluene was refluxed for 3 h (N2 atm.);; solvent was pumped off, ppt. was chromd. on silica gel with hexane-toluene;;

upstream raw materials:

allyltriphenylsilane

Downstream raw materials:

allyltriphenylsilane

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