2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside
CAS No.:663608-38-6
Molecular Formula:C₅₈H₅₁N₃O₁₈
Molecular Weight:1078.05
Hs Code.:

Synonyms:2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

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Chemical Property of 2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

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Technology Process of 2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

There total 4 articles about 2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 663608-37-5
2-chloroethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

: 663608-38-6
2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: With sodium azide; 18-crown-6 ether; In N,N-dimethyl-formamide; at 65 ℃; for 22h;
DOI:10.1023/A:1024905419008

Reference yield:

: 663608-36-4
4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

: 663608-38-6
2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / silver triflate / CH₂Cl₂ / 1 h / 20 °C

2: 86 percent / NaN₃; 18-crown-6 / dimethylformamide / 22 h / 65 °C

With sodium azide; 18-crown-6 ether; silver trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1023/A:1024905419008

Reference yield:

: 663608-35-3
1,2,3,6-tetra-O-benzoyl-4-O-(2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-D-glucopyranose

: 663608-38-6
2-azidoethyl 4-O-(4-O-acetyl-2,3,6-tri-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 18 h / 20 °C

2: 4.21 g / HBr; acetic acid / CH₂Cl₂ / 0.67 h / -10 °C

3: 91 percent / silver triflate / CH₂Cl₂ / 1 h / 20 °C

4: 86 percent / NaN₃; 18-crown-6 / dimethylformamide / 22 h / 65 °C

With pyridine; sodium azide; 18-crown-6 ether; hydrogen bromide; silver trifluoromethanesulfonate; acetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1023/A:1024905419008