C₃₃H₃₁FN₂O₉

Base Information

Chemical Name:C₃₃H₃₁FN₂O₉
CAS No.:1402416-09-4
Molecular Formula:C₃₃H₃₁FN₂O₉
Molecular Weight:618.616
Hs Code.:

C<sub>33</sub>H<sub>31</sub>FN<sub>2</sub>O<sub>9</sub>

Synonyms:C₃₃H₃₁FN₂O₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₁FN₂O₉

Chemical Property:

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Technology Process of C₃₃H₃₁FN₂O₉

There total 5 articles about C₃₃H₃₁FN₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₄₆N₂O₉Si

: 1402416-09-4
C₃₃H₃₁FN₂O₉

Guidance literature:: With sodium hydrogencarbonate; Selectfluor; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja307497h

Reference yield:

: 1266547-49-2
2,3-dibromo-5,8-di(methoxymethyloxy)naphthoquinone

: 1402416-09-4
C₃₃H₃₁FN₂O₉

Guidance literature:: Multi-step reaction with 5 steps

1: tris(diethylamino)sulfonium difluorotrimethylsiliconate / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

2: palladium diacetate; triphenylphosphine; silver carbonate / toluene / 2 h / 80 °C / Inert atmosphere

3: dmap; triflic azide / hexane; acetonitrile / 2 h / -30 - 24 °C / Inert atmosphere

4: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

5: sodium hydrogencarbonate; Selectfluor / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With dmap; triflic azide; tris(diethylamino)sulfonium difluorotrimethylsiliconate; palladium diacetate; sodium hydrogencarbonate; Selectfluor; triethylamine; triphenylphosphine; silver carbonate; In tetrahydrofuran; hexane; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja307497h

Reference yield:

: 1402416-07-2
C₃₃H₃₅BrO₉

: 1402416-09-4
C₃₃H₃₁FN₂O₉

Guidance literature:: Multi-step reaction with 4 steps

1: palladium diacetate; triphenylphosphine; silver carbonate / toluene / 2 h / 80 °C / Inert atmosphere

2: dmap; triflic azide / hexane; acetonitrile / 2 h / -30 - 24 °C / Inert atmosphere

3: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

4: sodium hydrogencarbonate; Selectfluor / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With dmap; triflic azide; palladium diacetate; sodium hydrogencarbonate; Selectfluor; triethylamine; triphenylphosphine; silver carbonate; In tetrahydrofuran; hexane; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja307497h