C₂₆H₂₆FN₃O₅S

Base Information

Chemical Name:C₂₆H₂₆FN₃O₅S
CAS No.:1311388-07-4
Molecular Formula:C₂₆H₂₆FN₃O₅S
Molecular Weight:511.574
Hs Code.:

C<sub>26</sub>H<sub>26</sub>FN<sub>3</sub>O<sub>5</sub>S

Synonyms:C₂₆H₂₆FN₃O₅S

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Chemical Property of C₂₆H₂₆FN₃O₅S

Chemical Property:

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Technology Process of C₂₆H₂₆FN₃O₅S

There total 5 articles about C₂₆H₂₆FN₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1311388-05-2
C₂₁H₁₈FN₃O₃S

: 1311388-07-4
C₂₆H₂₆FN₃O₅S

Guidance literature:: With dmap; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 79110-05-7
1-(2-fluoro-5-nitrophenyl)ethanone

: 1311388-07-4
C₂₆H₂₆FN₃O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 3 h / 85 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

2.2: 5 h / -78 °C

3.1: hydrogenchloride / methanol / 1.75 h / 20 °C

4.1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere; Cooling with ice

5.1: sulfuric acid / 1 h / Cooling with ice

6.1: dmap / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; titanium(IV) tetraethanolate; sulfuric acid; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;

Reference yield:

: 1311388-01-8
N-(1-(2-fluoro-5-nitrophenyl)ethylidene)-2-methylpropane-2-sulfinamide

: 1311388-07-4
C₂₆H₂₆FN₃O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

1.2: 5 h / -78 °C

2.1: hydrogenchloride / methanol / 1.75 h / 20 °C

3.1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere; Cooling with ice

4.1: sulfuric acid / 1 h / Cooling with ice

5.1: dmap / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; sulfuric acid; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;