2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Base Information

Chemical Name:2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
CAS No.:203253-68-3
Molecular Formula:C₁₉H₂₇BrO₂
Molecular Weight:367.326
Hs Code.:

Synonyms:2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Technology Process of 2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

There total 1 articles about 2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 65253-04-5
(-)-8-phenylmenthol

: 563-76-8
α-bromopropionyl bromide

: 203253-68-3
2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: With N,N-dimethyl-aniline; In diethyl ether; 1.) 0 deg C, 3 h, 2.) reflux, 3 h;
DOI:10.1039/a707310k

Reference yield: 80.0%

: 203253-68-3
2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 2-Nitro-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: With 3,5-dihydroxyphenol; sodium nitrite; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/S0040-4039(99)00935-1

Reference yield:

: 203253-68-3
2-Bromo-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: (S)-2-Methyl-2-nitro-3-(4-nitro-phenyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaNO₂; phloroglucinol / dimethylformamide / 2 h / 20 °C

2: NaH / dimethylformamide / 1 h / 20 °C / Irradiation

With 3,5-dihydroxyphenol; sodium hydride; sodium nitrite; In N,N-dimethyl-formamide; 1: Substitution / 2: Substitution;
DOI:10.1016/S0040-4039(99)00935-1