(dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene

Base Information

Chemical Name:(dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene
CAS No.:133156-91-9
Molecular Formula:C₂₂H₂₃NO₂Si
Molecular Weight:361.516
Hs Code.:

Synonyms:(dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene

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Chemical Property of (dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene

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Technology Process of (dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene

There total 3 articles about (dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 90-01-7
salicylic alcohol

: 114499-75-1
(dimethylaminomethyl-2 phenyl)-1 phenylsilane

: 133156-91-9
(dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene

Guidance literature:: In tetrachloromethane; at 77 ℃; for 48h;
DOI:10.1016/0022-328X(90)80080-J

Reference yield:

: 103-83-3
N,N'-dimethylbenzylamine

: 133156-91-9
(dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) Et₂O, hexane, rt, 48 h, 2.) rt, 48 h

2: 88 percent / CCl₄ / 48 h / 77 °C

With n-butyllithium; In tetrachloromethane;
DOI:10.1016/0022-328X(90)80080-J

Reference yield:

: 694-53-1
phenylsilane

: 133156-91-9
(dimethylaminomethyl-2 phenyl)-2 phenyl-2 sila-2 dioxo-1,3 tetrahydro-1,2,3,4 naphtalene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) Et₂O, hexane, rt, 48 h, 2.) rt, 48 h

2: 88 percent / CCl₄ / 48 h / 77 °C

With n-butyllithium; In tetrachloromethane;
DOI:10.1016/0022-328X(90)80080-J