dibutyl phosphorocyanidite

Base Information

• Chemical Name: dibutyl phosphorocyanidite
• CAS No.: 122278-71-1
• Molecular Formula: C₉H₁₈NO₂P
• Molecular Weight: 203.221

Synonyms:dibutyl phosphorocyanidite

Chemical Property of dibutyl phosphorocyanidite

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dibutyl phosphorocyanidite

There total 1 articles about dibutyl phosphorocyanidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

methyl thiocyanate (556-64-9) + diphosphorous acid tetrabutyl ester (54305-86-1) → O,O-dibutyl S-methyl phosphorothioate (20822-30-4) + dibutyl phosphorocyanidite (122278-71-1)

Guidance literature:

at 100 ℃; for 2h;

Reference yield: 82.0%

dibutyl phosphorocyanidite (122278-71-1) + tri-n-butyl-tin hydride (688-73-3) → dibutyl phosphonite (30653-71-5)

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 24h;

DOI:10.1007/BF00958064

upstream raw materials:

methyl thiocyanate

diphosphorous acid tetrabutyl ester

Downstream raw materials:

dibutyl phosphonite

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