4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride

Base Information

Chemical Name:4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride
CAS No.:66264-59-3
Molecular Formula:C₂₁H₂₅NO₄S*ClH
Molecular Weight:423.961
Hs Code.:

Synonyms:4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride

Chemical Property:

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Technology Process of 4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride

There total 4 articles about 4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-13-1,23239-32-9
2-amino-1-(4-methyoxyphenyl)propane

: 66264-58-2
2-bromo-4'-hydroxy-3'-(methylthio)acetophenone 4'-acetate

: 66264-59-3
4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride

Guidance literature:: With hydrogenchloride; triethylamine; In water; N,N-dimethyl-formamide;

Reference yield:

: 66264-57-1
4'-hydroxy-3'-(methylthio)acetophenone 4'-acetate

: 66264-59-3
4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; calcium carbonate / chloroform

2: hydrogenchloride; triethylamine / water; N,N-dimethyl-formamide

With hydrogenchloride; bromine; triethylamine; calcium carbonate; In chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 66264-55-9
4'-hydroxy-3'-mercaptoacetophenone

: 66264-59-3
4'-hydroxy-2-{[2-(4-methoxyphenyl)-1-methylethyl]amino}-3'-(methylthio)acetophenone 4'-acetate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / chloroform; acetone; benzene

2: triethylamine / dichloromethane

3: bromine; calcium carbonate / chloroform

4: hydrogenchloride; triethylamine / water; N,N-dimethyl-formamide

With hydrogenchloride; bromine; potassium carbonate; triethylamine; calcium carbonate; In dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetone; benzene;