ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate

Base Information

Chemical Name:ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate
CAS No.:1252021-79-6
Molecular Formula:C₂₉H₃₈O₃Si
Molecular Weight:462.704
Hs Code.:

Synonyms:ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate

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Technology Process of ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate

There total 1 articles about ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1252021-78-5
C₂₉H₃₆O₃Si

: 1252021-79-6
ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate

Guidance literature:: With sodium tetrahydroborate; nickel (II) chloride hexahydrate; In methanol; at 0 ℃;
DOI:10.1016/j.tetlet.2010.07.088

Reference yield: 95.0%

: 3112-85-4
methylphenylsulfonate

: 1252021-79-6
ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate

: 1252021-80-9
4-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)-1-(phenylsulfonyl)butan-2-one

Guidance literature:: methylphenylsulfonate; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;

ethyl 3-(1-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclohexa-2,5-dienyl)propanoate; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2010.10.076