(4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine

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Chemical Name:(4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine
CAS No.:439615-14-2
Molecular Formula:C₈₀H₁₃₅I₂NO₂S
Molecular Weight:1428.83
Hs Code.:

Synonyms:(4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine

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Chemical Property of (4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine

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Technology Process of (4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine

There total 5 articles about (4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: [4-(hexadecane-1-sulfonyl)-benzyl]-phosphonic acid diethyl ester

: 439615-12-0
4-{hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amino}-benzaldehyde

: 439615-14-2
(4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine

Guidance literature:: 4-{hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amino}-benzaldehyde; With sodium hydride; In 1,2-dimethoxyethane; at 20 ℃; for 0.333333h;

[4-(hexadecane-1-sulfonyl)-benzyl]-phosphonic acid diethyl ester; In 1,2-dimethoxyethane; at 90 ℃; Further stages.;
DOI:10.1021/ma020078v

Reference yield:

: 439615-11-9
hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-phenyl-amine

: 439615-14-2
(4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: phosphorus oxychloride / 2 h / 0 - 20 °C

1.2: 75 percent / dimethylformamide / 90 °C

2.1: NaH / 1,2-dimethoxy-ethane / 0.33 h / 20 °C

2.2: 75 percent / 1,2-dimethoxy-ethane / 90 °C

With sodium hydride; trichlorophosphate; In 1,2-dimethoxyethane;
DOI:10.1021/ma020078v

Reference yield:

: 4439-42-3
hexadecyl(phenyl)amine

: 439615-14-2
(4-{2-[4-(hexadecane-1-sulfonyl)-phenyl]-vinyl}-phenyl)-hexadecyl-[12-(4-hexadecyl-2,5-diiodo-phenyl)-dodecyl]-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / tetrabutylammonium bromide; sodium iodide; potassium carbonate / toluene / 48 h / Heating

2.1: phosphorus oxychloride / 2 h / 0 - 20 °C

2.2: 75 percent / dimethylformamide / 90 °C

3.1: NaH / 1,2-dimethoxy-ethane / 0.33 h / 20 °C

3.2: 75 percent / 1,2-dimethoxy-ethane / 90 °C

With tetrabutylammomium bromide; sodium hydride; potassium carbonate; sodium iodide; trichlorophosphate; In 1,2-dimethoxyethane; toluene;
DOI:10.1021/ma020078v