[4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine

Base Information

• Chemical Name: [4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine
• CAS No.: 852054-23-0
• Molecular Formula: C₂₂H₁₈F₂₁N
• Molecular Weight: 695.358

Synonyms:[4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine

Chemical Property of [4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine

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Technology Process of [4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine

There total 2 articles about [4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

[4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-carbamic acid tert-butyl ester (852054-15-0) → [4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine (852054-23-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jo048051s

Reference yield:

[4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodec-1-enyl)-benzyl]-propyl-carbamic acid tert-butyl ester → [4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine (852054-23-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / H₂ / Pd/C / ethyl acetate / 24 h / 20 °C / 2327.17 - 2585.74 Torr

2: 93 percent / CF₃COOH / CH₂Cl₂ / 2 h / 20 °C

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;

DOI:10.1021/jo048051s

Reference yield: 99.0%

[4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-amine (852054-23-0) + 2-trifluoromethyl-4-iodobenzenediazonium tetrafluoroborate → C29H20F24IN3

Guidance literature:

With potassium carbonate; In tetrahydrofuran; acetonitrile; at 0 - 20 ℃;

DOI:10.1021/jo048051s

upstream raw materials:

[4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluoro-dodecyl)-benzyl]-propyl-carbamic acid tert-butyl ester

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