N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

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Chemical Name:N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide
CAS No.:1205589-11-2
Molecular Formula:C₄₈H₄₈N₂O₆
Molecular Weight:748.919
Hs Code.:

Synonyms:N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

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Chemical Property of N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

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Technology Process of N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

There total 4 articles about N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4-(1,3-dioxolan-2-yl)-4-methylbenzylamine

: 130296-37-6
N-(1-hexylheptyl)-perylene-3,4,9,10-tetracarboxylic-3,4-carboximide-9,10-anhydride

: 1205589-11-2
N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: With 1H-imidazole; hydrogenchloride; In ethanol; water; at 140 ℃; for 3h;

Reference yield: 70.0%

: 66522-61-0
(4-(2-methyl-1,3-dioxolan-2-yl)phenyl)methanamine

: 130296-37-6
N-(1-hexylheptyl)-perylene-3,4,9,10-tetracarboxylic-3,4-carboximide-9,10-anhydride

: 1205589-11-2
N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: With 1H-imidazole; at 140 ℃;
DOI:10.1002/chem.200901839

Reference yield:

: 4-(1,3-dioxolan-2-yl)-4-methylbenzonitrile

: 1205589-11-2
N-[4-(2-methyl[1,3]dioxolan-2-yl)benzyl]-N’-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 18.25 h / 0 - 20 °C / Inert atmosphere

2: hydrogenchloride; 1H-imidazole / ethanol; water / 3 h / 140 °C

With 1H-imidazole; hydrogenchloride; lithium aluminium tetrahydride; In diethyl ether; ethanol; water;