(6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde

Base Information

• Chemical Name: (6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde
• CAS No.: 886552-41-6
• Molecular Formula: C₁₇H₂₃N₃O₅
• Molecular Weight: 349.387

Synonyms:(6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde

Chemical Property of (6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde

Chemical Property:

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Technology Process of (6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde

There total 1 articles about (6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

3-(6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-1-propene (848618-22-4) → (6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde (886552-41-6)

Guidance literature:

With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; In 1,4-dioxane; water; tert-butyl alcohol; at 20 ℃; for 0.5h;

DOI:10.1021/jo052489q

Reference yield: 84.0%

(6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde (886552-41-6) → (6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methoxy-β-D-glucopyranosyl)-acetaldehyde (886552-55-2)

Guidance literature:

With zinc diacetate; sodium methylate; In methanol; at 20 ℃; for 72h;

DOI:10.1021/jo052489q

Reference yield:

(6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-acetaldehyde (886552-41-6) → (3E,12E)-(1R,6R,7S,8R,9R,10R,15R,16S,17R,18R)-8,17-Bis-benzyloxy-7,9,16,18-tetramethoxy-19,20-dioxa-3,12-diaza-tricyclo[13.3.1.16,10]icosa-3,12-diene (886552-43-8)

Guidance literature:

With polymer-bound diphenylphosphine; In tetrahydrofuran; at 20 ℃; for 20h;

DOI:10.1021/jo052489q

upstream raw materials:

3-(6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methyl-α-D-glucopyranosyl)-1-propene

Downstream raw materials:

(6'-azido-3'-O-benzyl-6'-deoxy-2',4'-di-O-methoxy-β-D-glucopyranosyl)-acetaldehyde

(3E,12E)-(1R,6R,7S,8R,9R,10R,15R,16S,17R,18R)-8,17-Bis-benzyloxy-7,9,16,18-tetramethoxy-19,20-dioxa-3,12-diaza-tricyclo[13.3.1.1^6,10]icosa-3,12-diene

(3E,12E)-(1R,6S,7S,8R,9R,10R,15S,16S,17R,18R)-8,17-Bis-benzyloxy-7,9,16,18-tetramethoxy-19,20-dioxa-3,12-diaza-tricyclo[13.3.1.1^6,10]icosa-3,12-diene

(1R,6S,7S,8R,9R,10R,15S,16S,17R,18R)-8,17-Bis-benzyloxy-7,9,16,18-tetramethoxy-19,20-dioxa-3,12-diaza-tricyclo[13.3.1.1^6,10]icosane

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