3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 1395897-59-2
• Molecular Formula: C₂₁H₁₃BCl₂F₂N₂
• Molecular Weight: 413.061

Synonyms:3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property of 3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

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Technology Process of 3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 3 articles about 3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

8-(2,6-dichlorophen-1-yl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1269636-16-9) + benzenediazonium tetrafluoroborate (369-57-3) → 3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1395897-59-2)

Guidance literature:

With ferrocene; In acetone; at 20 ℃; for 0.583333h; Inert atmosphere;

DOI:10.1002/anie.201410853

Reference yield: 46.0%

bromobenzene (108-86-1,52753-63-6) + 8-(2,6-dichlorophen-1-yl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1269636-16-9) → 3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1395897-59-2) + 3,5-diphenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1395897-66-1)

Guidance literature:

With tricyclohexylphosphine tetrafluoroborate; palladium diacetate; potassium carbonate; Trimethylacetic acid; In toluene; at 110 ℃; for 3.5h; Inert atmosphere;

DOI:10.1039/c2cc34549h

Reference yield: 42.0%

8-(2,6-dichlorophen-1-yl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1269636-16-9) + potassium phenyltrifluoborate → 3-phenyl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1395897-59-2)

Guidance literature:

With manganese(III) triacetate dihydrate; In N,N-dimethyl-formamide; at 50 ℃; for 22.5h;

DOI:10.1002/chem.201500938

upstream raw materials:

bromobenzene

8-(2,6-dichlorophen-1-yl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

benzenediazonium tetrafluoroborate

Downstream raw materials:

3-phenyl-5-thien-3-yl-8-(2,6-dichlorophenyl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

((C₆H₅)C₉H₄(C₆H₃Cl₂)N₂BF₂)2C₆H₄

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