C₆₀H₁₁₈O₁₀Si₅

Base Information

Chemical Name:C₆₀H₁₁₈O₁₀Si₅
CAS No.:912805-73-3
Molecular Formula:C₆₀H₁₁₈O₁₀Si₅
Molecular Weight:1140.02
Hs Code.:

C<sub>60</sub>H<sub>118</sub>O<sub>10</sub>Si<sub>5</sub>

Synonyms:C₆₀H₁₁₈O₁₀Si₅

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Chemical Property of C₆₀H₁₁₈O₁₀Si₅

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Technology Process of C₆₀H₁₁₈O₁₀Si₅

There total 18 articles about C₆₀H₁₁₈O₁₀Si₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 912805-73-3
C₆₀H₁₁₈O₁₀Si₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaH / tetrahydrofuran

1.2: 70 percent / n-BuLi

2.1: 100 percent / hydrogen / Ru₂Cl₂[(R)-BINAP]2*Et₃N / methanol / 66 h / 23 °C / 42923.3 Torr

3.1: 99 percent / imidazole / dimethylformamide / 15 h / 23 °C

4.1: 93 percent / DIBAL-H / petroleum ether; toluene / 0.08 h / -78 °C

5.1: n-butyllithium; potassium tert-butoxide / petroleum ether; tetrahydrofuran / -78 - -45 °C

5.2: boron trifluoride diethyl etherate / (+)-B-methoxydiisopinocamphenylborane / petroleum ether; tetrahydrofuran; diethyl ether / -78 °C

5.3: petroleum ether; tetrahydrofuran; diethyl ether / 8.5 h

6.1: 66.2 mg / 4-(dimethylamino)pyridine / toluene / 1.5 h / 23 °C

With 1H-imidazole; dmap; n-butyllithium; potassium tert-butylate; hydrogen; sodium hydride; diisobutylaluminium hydride; Ru₂Cl₂[(R)-BINAP]2*Et₃N; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; Petroleum ether; 6.1: Yamaguchi esterification;
DOI:10.1021/ja062364i

Reference yield:

: 2,3,5-tri-O-(tert-butyldimethylsilyl)-L-arabinofuranose

: 912805-73-3
C₆₀H₁₁₈O₁₀Si₅

Guidance literature:: Multi-step reaction with 5 steps

1: diphenyl sulfoxide; 2,4,6-tri-tert-butylpyridine / CH₂Cl₂; toluene / 1.5 h / -78 - -45 °C

2: 119 mg / CH₂Cl₂; toluene / -78 - 0 °C

3: 77 percent / barium hydroxide octahydrate / methanol / 20.5 h / 20 °C

4: triethylamine / toluene / 1.5 h / 23 °C

5: 66.2 mg / 4-(dimethylamino)pyridine / toluene / 1.5 h / 23 °C

With dmap; barium hydroxide octahydrate; 2,4,6-tri-tertbutylpyridine; 1,1'-sulfinylbisbenzene; triethylamine; In methanol; dichloromethane; toluene; 5: Yamaguchi esterification;
DOI:10.1021/ja062364i

Reference yield:

: 912805-68-6
isobutyl (3R)-5-benzyloxy-3-[(tert-butyldimethylsilyl)oxy]pentanoate

: 912805-73-3
C₆₀H₁₁₈O₁₀Si₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: 93 percent / DIBAL-H / petroleum ether; toluene / 0.08 h / -78 °C

2.1: n-butyllithium; potassium tert-butoxide / petroleum ether; tetrahydrofuran / -78 - -45 °C

2.2: boron trifluoride diethyl etherate / (+)-B-methoxydiisopinocamphenylborane / petroleum ether; tetrahydrofuran; diethyl ether / -78 °C

2.3: petroleum ether; tetrahydrofuran; diethyl ether / 8.5 h

3.1: 162 mg / CH₂Cl₂; toluene / 22.5 h / -45 - 23 °C

4.1: 94 percent / hydrogen / Pd/C / methanol / 1.3 h / 23 °C

5.1: 88 percent / sodium periodate; ruthenium chloride hydrate / acetonitrile; CCl₄; H₂O / 0.5 h / 23 °C

6.1: triethylamine / toluene / 1.5 h / 23 °C

7.1: 66.2 mg / 4-(dimethylamino)pyridine / toluene / 1.5 h / 23 °C

With dmap; ruthenium trichloride; sodium periodate; n-butyllithium; potassium tert-butylate; hydrogen; diisobutylaluminium hydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water; toluene; acetonitrile; Petroleum ether; 7.1: Yamaguchi esterification;
DOI:10.1021/ja062364i