(1,3-di-tert-butylimidazol-2-ylidene)CH₂CH=(C₅H₄N)Al(C₆F₅)₃

Base Information

• Chemical Name: (1,3-di-tert-butylimidazol-2-ylidene)CH₂CH=(C₅H₄N)Al(C₆F₅)₃
• CAS No.: 1632067-29-8
• Molecular Formula: C₃₆H₂₇AlF₁₅N₃
• Molecular Weight: 813.588
• Mol file: 1632067-29-8.mol

Synonyms:(1,3-di-tert-butylimidazol-2-ylidene)CH₂CH=(C₅H₄N)Al(C₆F₅)₃

Chemical Property of (1,3-di-tert-butylimidazol-2-ylidene)CH₂CH=(C₅H₄N)Al(C₆F₅)₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1,3-di-tert-butylimidazol-2-ylidene)CH₂CH=(C₅H₄N)Al(C₆F₅)₃

There total 3 articles about (1,3-di-tert-butylimidazol-2-ylidene)CH₂CH=(C₅H₄N)Al(C₆F₅)₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C18AlF15*C7H7N + 1,3-di-tert-butylimidazol-2-ylidene (157197-53-0) → (1,3-di-tert-butylimidazol-2-ylidene)CH2CH=(C5H4N)Al(C6F5)3 (1632067-29-8)

Guidance literature:

In toluene; at 20 ℃;

DOI:10.1021/ma5019389

Reference yield:

(2-vinylpyridine)Al(C6F5)3 (1632067-27-6) + 1,3-di-tert-butylimidazol-2-ylidene (157197-53-0) → (1,3-di-tert-butylimidazol-2-ylidene)CH2CH=(C5H4N)Al(C6F5)3 (1632067-29-8)

Guidance literature:

In benzene-d6; at 25 ℃; for 0.166667h; Sealed tube;

DOI:10.1055/s-0033-1341248

Reference yield:

2-vinylpyridine (100-69-6,25014-15-7,27476-03-5,329041-71-6) → (1,3-di-tert-butylimidazol-2-ylidene)CH2CH=(C5H4N)Al(C6F5)3 (1632067-29-8)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 25 °C

2: benzene-d6 / 0.17 h / 25 °C / Sealed tube

In benzene-d6; toluene;

DOI:10.1055/s-0033-1341248

upstream raw materials:

(2-vinylpyridine)Al(C₆F₅)₃

1,3-di-tert-butylimidazol-2-ylidene

2-vinylpyridine