6-Hydroxyiminomethyl-3,5-di-(1',2'-oxazol-4'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin

Base Information

Chemical Name:6-Hydroxyiminomethyl-3,5-di-(1',2'-oxazol-4'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin
CAS No.:133615-45-9
Molecular Formula:C₁₈H₁₄N₄O₅S
Molecular Weight:398.399
Hs Code.:

Synonyms:6-Hydroxyiminomethyl-3,5-di-(1',2'-oxazol-4'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin

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Chemical Property of 6-Hydroxyiminomethyl-3,5-di-(1',2'-oxazol-4'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin

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Technology Process of 6-Hydroxyiminomethyl-3,5-di-(1',2'-oxazol-4'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin

There total 2 articles about 6-Hydroxyiminomethyl-3,5-di-(1',2'-oxazol-4'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3,5-Di-(1'-dimethylamino-3'-dimethylimonio-prop-1'-en-2'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin-6-aldehyd-diperchlorat

: 133615-45-9
6-Hydroxyiminomethyl-3,5-di-(1',2'-oxazol-4'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In water; acetic acid; for 3h; Heating;

Reference yield:

: 37091-40-0
2,4-Dimethyl-N-(4-methyl-phenyl)-buta-1,3-dien-1,4-sultam

: 133615-45-9
6-Hydroxyiminomethyl-3,5-di-(1',2'-oxazol-4'-yl)-1,1-dioxo-2-(p-tolyl)-1,2-thiazin

Guidance literature:: Multi-step reaction with 2 steps

1: 1) POCl₃, 2) NaClO₄, H₂O / 1) 0 deg C, 2) r.t.

2: 90 percent / NH₂OH*HCl, sodium acetate / acetic acid; H₂O / 3 h / Heating

With hydroxylamine hydrochloride; sodium perchlorate; water; sodium acetate; trichlorophosphate; In water; acetic acid;