Technology Process of C65H99Cl2N3O16S
There total 7 articles about C65H99Cl2N3O16S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C46H79NO14S2;
With
tributylphosphine; water;
In
N,N-dimethyl-formamide;
at 20 ℃;
Inert atmosphere;
3-cyclopentyloxy-4-methoxy-phenylamine;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 20h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dichloromethane / 7 h / 20 °C / Molecular sieve
2.1: tributylphosphine; water / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2.2: 20 h / 20 °C / Inert atmosphere
With
tributylphosphine; water;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium cyanoborohydride; acetic acid / methanol; water / 5 h / 28 °C
2.1: tributylphosphine; water / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2.2: 20 h / 20 °C / Inert atmosphere
With
tributylphosphine; water; sodium cyanoborohydride; acetic acid;
In
methanol; water; N,N-dimethyl-formamide;