(1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol

Base Information

Chemical Name:(1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol
CAS No.:942616-27-5
Molecular Formula:C₂₅H₃₁NO₃Si
Molecular Weight:421.612
Hs Code.:

Synonyms:(1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol

Chemical Property:

Purity/Quality:

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Technology Process of (1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol

There total 2 articles about (1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 942617-73-4
1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropanecarboxylic acid ethyl ester

: 942616-27-5
(1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at -15 - -5 ℃; for 1.91667h; Product distribution / selectivity;

Reference yield:

: 942617-72-3
1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropanecarboxylic acid methyl ester

: 942616-27-5
(1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 - 10 ℃; Product distribution / selectivity;

Reference yield:

: 942616-27-5
(1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol

: 4023-34-1
cyclopropanecarboxylic acid chloride

: C₂₃H₂₁NO₄

Guidance literature:: (1-{3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-4-phenyl-isoxazol-5-yl}-cyclopropyl)-methanol; cyclopropanecarboxylic acid chloride; With triethylamine; In dichloromethane; at 20 - 40 ℃;

In dichloromethane;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1.5h;