2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine

Base Information

Chemical Name:2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine
CAS No.:1352035-53-0
Molecular Formula:C₂₅H₂₄N₄O₂
Molecular Weight:412.491
Hs Code.:

Synonyms:2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine

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Chemical Property of 2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine

Chemical Property:

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Technology Process of 2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine

There total 5 articles about 2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352036-32-8
C₃₅H₄₀N₄O₆

: 1352035-53-0
2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.10.009

Reference yield:

: 1352036-30-6
3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinoline-1-carbaldehyde

: 1352035-53-0
2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol / 1 h / 20 °C / Inert atmosphere

2: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 3 h / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; triphenylphosphine; trifluoroacetic acid; In ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmc.2012.10.009

Reference yield:

: 1352036-31-7
3-([1,1-biphenyl]-3-yl)-6,7-dimethoxy-1-hydroxymethylisoquinoline

: 1352035-53-0
2-((3-([1,1'-biphenyl]-3-yl)-6,7-dimethoxyisoquinolin-1-yl)methyl)guanidine

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 3 h / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; triphenylphosphine; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1016/j.bmc.2012.10.009