(+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane

Base Information

Chemical Name:(+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane
CAS No.:112168-48-6
Molecular Formula:C₁₄H₁₅NO₇
Molecular Weight:309.276
Hs Code.:

Synonyms:(+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane

Suppliers and Price of (+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane

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Technology Process of (+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane

There total 3 articles about (+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34638-25-0,38110-77-9,43119-28-4,54483-22-6,26054-46-6
(1R,5S)-2-oxabicyclo[3.3.0]oct-6-en-3-one

: 112168-48-6
(+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane

Guidance literature:: Multi-step reaction with 3 steps

1: 55.2 percent / KClO₃ / OsO₄ / H₂O / 20.5 h

2: 82 percent / p-toluene sulphonic acid / benzene / 0.33 h / Heating

3: 1.) NaOH/H₂O; 2.) acid

With sodium hydroxide; potassium chlorate; water; toluene-4-sulfonic acid; osmium(VIII) oxide; In water; benzene;

Reference yield:

: 112318-61-3
(+)-2β,3β,5β-trihydroxycyclopentyl-1β-acetic acid γ-lactone

: 112168-48-6
(+)-1β-carboxymethyl-5β-hydroxy-2β,3β-(p-nitrobenzylidene) dioxycyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / p-toluene sulphonic acid / benzene / 0.33 h / Heating

2: 1.) NaOH/H₂O; 2.) acid

With sodium hydroxide; water; toluene-4-sulfonic acid; In benzene;