Technology Process of C13H25NO3Si
There total 1 articles about C13H25NO3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 1H-imidazole / dichloromethane / 0 °C
2.1: tert-butylhypochlorite / diethyl ether / 0.5 h / 0 °C
2.2: 0.5 h / 0 - 20 °C
3.1: 2,6-dimethylpyridine / dichloromethane / -10 - 40 °C
4.1: copper(I) bromide dimethylsulfide complex / diethyl ether / 0.75 h / -50 - -25 °C / Inert atmosphere
4.2: 0.75 h / -50 - -40 °C
5.1: hydrogen / palladium 10% on activated carbon / methanol / -50 - -25 °C / 2068.65 Torr
6.1: tert-butylhypochlorite / diethyl ether / 0.33 h / 0 °C
With
1H-imidazole; 2,6-dimethylpyridine; copper(I) bromide dimethylsulfide complex; tert-butylhypochlorite; hydrogen;
palladium 10% on activated carbon;
In
methanol; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran / 5 h / -40 - 20 °C
2.1: sodium carbonate / water / 1.25 h / 20 °C
3.1: lithium hydroxide / water; methanol / 20 °C
3.2: pH 2
4.1: potassium tert-butylate / dimethyl sulfoxide / 0.25 h / 20 °C
4.2: 2 h
With
potassium tert-butylate; sodium tris(acetoxy)borohydride; sodium carbonate; acetic acid; lithium hydroxide;
In
tetrahydrofuran; methanol; water; dimethyl sulfoxide;
