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Technology Process of [Os(C=C(CPh2CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr3)2]BF4

[Os(C=C(CPh2CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr3)2]BF4

Base Information
  • Chemical Name:[Os(C=C(CPh2CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr3)2]BF4
  • CAS No.:883910-14-3
  • Molecular Formula:BF4*C47H74N3OsP2
  • Molecular Weight:1020.08
  • Hs Code.:
[Os(C=C(CPh<sub>2</sub>CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr<sub>3</sub>)2]BF<sub>4</sub>

Synonyms:[Os(C=C(CPh2CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr3)2]BF4

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Chemical Property of [Os(C=C(CPh2CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr3)2]BF4
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Technology Process of [Os(C=C(CPh2CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr3)2]BF4

There total 1 articles about [Os(C=C(CPh2CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr3)2]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

[Os((E)-CH=CHCy)(=C=C=CPh<sub>2</sub>)(acetonitrile)2(P(i)Pr<sub>3</sub>)2]BF<sub>4</sub>

[Os((E)-CH=CHCy)(=C=C=CPh2)(acetonitrile)2(P(i)Pr3)2]BF4

acetonitrile
75-05-8,26809-02-9

acetonitrile

[Os(C=C(CPh<sub>2</sub>CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr<sub>3</sub>)2]BF<sub>4</sub>
883910-14-3

[Os(C=C(CPh2CCy=CH(cyclic))CMe=NH(cyclic)(acetonitrile)2(P(i)Pr3)2]BF4

Guidance literature:
In acetonitrile; Schlenk technique; soln. of osmium complex in acetonitrile refluxed for 8 h; filtration through Celite, filtrate evapd., addn. of Et2O, solid washed with Et2O, dried under vac.; elem. anal.;
DOI:10.1021/ja058355b
upstream raw materials:

acetonitrile

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