(2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester

Base Information

Chemical Name:(2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester
CAS No.:78914-33-7
Molecular Formula:C₂₅H₂₆N₂O₆
Molecular Weight:450.491
Hs Code.:

Synonyms:(2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester

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Chemical Property of (2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester

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Technology Process of (2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester

There total 1 articles about (2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6506-31-6
dimethyl acetonedicarboxylate ethylene ketal

: 112616-41-8
N-benzyl-3(o-amino)phenyl pyrrolidine-2,5-dione

: 78914-33-7
(2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester

Guidance literature:: With diisobutylaluminium hydride; Multistep reaction;
DOI:10.1021/ja00405a089

Reference yield:

: 78914-33-7
(2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester

: C₂₄H₂₆N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) t-BuONa, t-BuOH / 1.) room temperature, 2.) room temperature

2: NaBH₄/H+

3: HCl, CH₃OH / 0.5 h / Heating

With hydrogenchloride; methanol; sodium tetrahydroborate; hydrogen cation; sodium t-butanolate; tert-butyl alcohol;
DOI:10.1021/ja00405a089

Reference yield:

: 78914-33-7
(2-{2-[(E)-2-(1-Benzyl-2,5-dioxo-pyrrolidin-3-yl)-phenylimino]-ethyl}-[1,3]dioxolan-2-yl)-acetic acid methyl ester

: 78954-15-1
(3aS,6aR,11bR)-3-Benzyl-5-hydroxy-2-oxo-2,3,3a,6,6a,7-hexahydro-1H-pyrrolo[2,3-d]carbazole-4-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) t-BuONa, t-BuOH / 1.) room temperature, 2.) room temperature

2: NaBH₄/H+

3: HCl, CH₃OH / 0.5 h / Heating

With hydrogenchloride; methanol; sodium tetrahydroborate; hydrogen cation; sodium t-butanolate; tert-butyl alcohol;
DOI:10.1021/ja00405a089