2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester

Base Information

Chemical Name:2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester
CAS No.:872462-87-8
Molecular Formula:C₆₀H₆₃NO₁₁
Molecular Weight:974.16
Hs Code.:

Synonyms:2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester

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Chemical Property of 2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester

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Technology Process of 2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester

There total 2 articles about 2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: TAM-acid-methyl ester(Bn)2

: 156536-14-0
2-amino-1,3-bis(1,3-dibenzyl-2-glyceroxy)-2-propane

: 872462-87-8
2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester

Guidance literature:: TAM-acid-methyl ester(Bn)2; With oxalyl dichloride; N,N-dimethyl-formamide; In toluene; at 60 ℃; for 4h;

2-amino-1,3-bis(1,3-dibenzyl-2-glyceroxy)-2-propane; With triethylamine; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield: 89.0%

: C₂₃H₁₉ClO₅

: 156536-14-0
2-amino-1,3-bis(1,3-dibenzyl-2-glyceroxy)-2-propane

: 872462-87-8
2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 16h;

Reference yield: 96.0%

: 872462-87-8
2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester

: 872462-88-9
2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide

Guidance literature:: 2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide methylester; With potassium hydroxide; In methanol; water; for 6h; Heating / reflux;

With hydrogenchloride; In water; pH=1;