N-(dimethylamino)ethyl-4-(2'-aminomethyl-1',6'-dimethyl-3'-benxyloxy-4'-pyridinone)-1,8-naphthalimide

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Chemical Name:N-(dimethylamino)ethyl-4-(2'-aminomethyl-1',6'-dimethyl-3'-benxyloxy-4'-pyridinone)-1,8-naphthalimide
CAS No.:1430836-79-5
Molecular Formula:C₃₁H₃₂N₄O₄
Molecular Weight:524.619
Hs Code.:

Synonyms:N-(dimethylamino)ethyl-4-(2'-aminomethyl-1',6'-dimethyl-3'-benxyloxy-4'-pyridinone)-1,8-naphthalimide

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Chemical Property of N-(dimethylamino)ethyl-4-(2'-aminomethyl-1',6'-dimethyl-3'-benxyloxy-4'-pyridinone)-1,8-naphthalimide

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Technology Process of N-(dimethylamino)ethyl-4-(2'-aminomethyl-1',6'-dimethyl-3'-benxyloxy-4'-pyridinone)-1,8-naphthalimide

There total 2 articles about N-(dimethylamino)ethyl-4-(2'-aminomethyl-1',6'-dimethyl-3'-benxyloxy-4'-pyridinone)-1,8-naphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 182344-65-6
2-(6-bromo-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine

: (2-aminomethyl-3-benzyloxy-6-methyl-pyridin-4(1H)-one)

: 1430836-79-5
N-(dimethylamino)ethyl-4-(2'-aminomethyl-1',6'-dimethyl-3'-benxyloxy-4'-pyridinone)-1,8-naphthalimide

Guidance literature:: With potassium tert-butylate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In N,N-dimethyl-formamide; at 130 ℃; for 0.0833333h; Microwave irradiation;
DOI:10.1016/j.dyepig.2013.02.020

Reference yield:

: 81-86-7
4-bromo-1,8-naphthalenedicarboxylic anhydride

: 1430836-79-5
N-(dimethylamino)ethyl-4-(2'-aminomethyl-1',6'-dimethyl-3'-benxyloxy-4'-pyridinone)-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 4 h / Reflux

2: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; potassium tert-butylate / N,N-dimethyl-formamide / 0.08 h / 130 °C / Microwave irradiation

With potassium tert-butylate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In ethanol; N,N-dimethyl-formamide; 2: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.dyepig.2013.02.020