(2R,3S,4S,5R)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal

Base Information

Chemical Name:(2R,3S,4S,5R)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal
CAS No.:78136-21-7
Molecular Formula:C₄₀H₅₀O₆Si
Molecular Weight:654.919
Hs Code.:

Synonyms:(2R,3S,4S,5R)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal

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Chemical Property of (2R,3S,4S,5R)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal

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Technology Process of (2R,3S,4S,5R)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal

There total 7 articles about (2R,3S,4S,5R)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 175470-19-6
tert-Butyl-dimethyl-((1R,2S,3S,4R)-2,3,4-tris-benzyloxy-1-benzyloxymethyl-5,5-bis-ethylsulfanyl-pentyloxy)-silane

: 78136-21-7
(2R,3S,4S,5R)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal

Guidance literature:: With cadmium(II) carbonate; mercury dichloride; In acetone; for 1h;

Reference yield: 74.0%

: 78136-19-3,78184-88-0
(2S,3R,4S)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexan-1-ol

: 78136-20-6,78136-21-7
(2R,3S,4S)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; for 3h;
DOI:10.1016/S0008-6215(00)85231-3

Reference yield:

: 1045730-76-4
(3R,4R,5S)-1,3,4,5-Tetrakis-benzyloxy-6-trityloxy-hexan-2-ol

: 78136-20-6,78136-21-7
(2R,3S,4S)-2,3,4,6-Tetrakis-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-hexanal

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / imidazole / dimethylformamide / 48 h / 35 °C

2: 65 percent / 70 percent acetic acid / acetic acid / Heating

3: 74 percent / pyridinium chlorochromate, sodium acetate / CH₂Cl₂ / 3 h

With 1H-imidazole; sodium acetate; acetic acid; pyridinium chlorochromate; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85231-3