benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester

Base Information

Chemical Name:benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester
CAS No.:864237-85-4
Molecular Formula:C₁₇H₁₂Cl₂N₂O₅S
Molecular Weight:427.265
Hs Code.:

Synonyms:benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester

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Chemical Property of benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester

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Technology Process of benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester

There total 3 articles about benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 38383-43-6
2,4-dichlorophenoxy acetic acid ethylene glycol

: 35272-27-6
benzo[d][1,2,3]thiadiazole-7-carboxylic acid

: 864237-85-4
benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester

Guidance literature:: benzo[d][1,2,3]thiadiazole-7-carboxylic acid; With thionyl chloride;

2,4-dichlorophenoxy acetic acid ethylene glycol;
DOI:10.1021/jf203974p

Reference yield: 55.5%

: 38383-43-6
2,4-dichlorophenoxy acetic acid ethylene glycol

: 124371-49-9
benzothiadiazole-7-carboxylic acid chloride

: 864237-85-4
benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester

Guidance literature:: With triethylamine; In toluene; at 20 ℃; for 20.6h;

Reference yield:

: 94-75-7,89300-30-1
2,4-Dichlorophenoxyacetic acid

: 864237-85-4
benzo-1,2,3-thiadiazole-7-carboxylic acid 2-(2,4-dichlorophenoxyacetoxy)ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid

2: thionyl chloride

With thionyl chloride; sulfuric acid;
DOI:10.1021/jf203974p