methyl 2,4-di-O-benzyl-3-O-(2-O-acetyl-3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside

Base Information

• Chemical Name: methyl 2,4-di-O-benzyl-3-O-(2-O-acetyl-3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside
• CAS No.: 1012859-15-2
• Molecular Formula: C₄₄H₅₀O₁₀
• Molecular Weight: 738.875

Synonyms:methyl 2,4-di-O-benzyl-3-O-(2-O-acetyl-3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside

Chemical Property of methyl 2,4-di-O-benzyl-3-O-(2-O-acetyl-3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside

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Technology Process of methyl 2,4-di-O-benzyl-3-O-(2-O-acetyl-3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside

There total 1 articles about methyl 2,4-di-O-benzyl-3-O-(2-O-acetyl-3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

p-tolyl 2-O-acetyl-3,5-di-O-benzyl-1-thio-3-C-vinyl-α,β-L-lyxofuranoside + (2R,3R,4R,5R,6S)-3,5-Bis-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-ol (69850-47-1) → methyl 2,4-di-O-benzyl-3-O-(2-O-acetyl-3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside (1012859-15-2)

Guidance literature:

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃; for 0.666667h;

DOI:10.1016/j.carres.2007.10.035

Reference yield: 89.0%

methyl 2,4-di-O-benzyl-3-O-(2-O-acetyl-3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside (1012859-15-2) → methyl 2,4-di-O-benzyl-3-O-(3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside (1012859-18-5)

Guidance literature:

With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.carres.2007.10.035

upstream raw materials:

(2R,3R,4R,5R,6S)-3,5-Bis-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-ol

Downstream raw materials:

methyl 2,4-di-O-benzyl-3-O-(3,5-di-O-benzyl-3-C-vinyl-α-L-lyxofuranosyl)-α-L-rhamnopyranoside

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