4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

Base Information

Chemical Name:4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin
CAS No.:100046-11-5
Molecular Formula:C₄₄H₄₆N₄O₈
Molecular Weight:758.871
Hs Code.:

Synonyms:4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

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Chemical Property of 4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

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Technology Process of 4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

There total 1 articles about 4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 100082-69-7
4,6-bis(2-acetoxyethyl)-8-<(benzyloxy)carbonyl>-1-<2-(methoxycarbonyl)ethyl>-1',2,3,5,7,-pentamethyl-a,c-biladiene dihydrobromide

: 100046-11-5
4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

Guidance literature:: With bromine; iodine; In 1,2-dichloro-benzene; for 0.333333h; Heating;
DOI:10.1021/jo00355a015

Reference yield: 94.0%

: 100046-11-5
4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

: 100046-12-6
6-<(benzyloxy)carbonyl>-2,4-bis(2-hydroxyethyl)-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

Guidance literature:: With sulfuric acid; In methanol; for 1h; Ambient temperature;
DOI:10.1021/jo00355a015

Reference yield:

: 100046-11-5
4,6-bis(2-acetoxyethyl)-6-<(benzyloxy)carbonyl>-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

: 100046-13-7
6-<(benzyloxy)carbonyl>-2,4-bis(2-chloroethyl)-7-<2-(methoxycarbonyl)ethyl>-1,3,5,8,-tetramethylporphyrin

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / concd H₂SO₄ / methanol / 1 h / Ambient temperature

2: 90 percent / K₂CO₃, SOCl₂ / CHCl₃; dimethylformamide / 1 h / Ambient temperature

With thionyl chloride; sulfuric acid; potassium carbonate; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00355a015