di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate

Base Information

Chemical Name:di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate
CAS No.:132464-56-3
Molecular Formula:C₂₂H₃₈BNO₄
Molecular Weight:391.359
Hs Code.:

Synonyms:di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate

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Chemical Property of di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate

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Technology Process of di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate

There total 1 articles about di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 688-74-4
boric acid tributyl ester

: 132464-55-2
N,N-diethyl 3-isopropoxybenzamide

: 132464-56-3
di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; dropwise addn. of a soln. of the benzamide in THF to a stirred soln. of s-BuLi and TMEDA in THF at -78°C; stirring at -78°C for 2 h; addn. of tributyl borate; stirring below -40°C for 4 h; quenching with NH4Cl soln. at -40°C;; short-path distn.; elem. anal.;;
DOI:10.1139/v94-035