7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.2^5,8.0^1,5.0^10,15.0^16,21]tricosa-6,10,12,14,16,18,20,22-octaene

Base Information

• Chemical Name: 7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.2^5,8.0^1,5.0^10,15.0^16,21]tricosa-6,10,12,14,16,18,20,22-octaene
• CAS No.: 496839-79-3
• Molecular Formula: C₃₆H₃₀O₃
• Molecular Weight: 510.632

Synonyms:7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.2^5,8.0^1,5.0^10,15.0^16,21]tricosa-6,10,12,14,16,18,20,22-octaene

Chemical Property of 7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.2^5,8.0^1,5.0^10,15.0^16,21]tricosa-6,10,12,14,16,18,20,22-octaene

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Technology Process of 7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.2^5,8.0^1,5.0^10,15.0^16,21]tricosa-6,10,12,14,16,18,20,22-octaene

There total 2 articles about 7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.2^5,8.0^1,5.0^10,15.0^16,21]tricosa-6,10,12,14,16,18,20,22-octaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

9-{[3,5-bis(benzyloxy)benzyloxy]methyl}anthracene (496839-75-9) → 7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.25,8.01,5.010,15.016,21]tricosa-6,10,12,14,16,18,20,22-octaene (496839-79-3)

Guidance literature:

In benzene; Irradiation;

DOI:10.1016/S0040-4039(02)01476-4

Reference yield:

3,5-dibenzyloxybenzyl alcohol (24131-31-5) → 7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.25,8.01,5.010,15.016,21]tricosa-6,10,12,14,16,18,20,22-octaene (496839-79-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / Bu₄NBr / chlorobenzene; H₂O

2: 100 percent / benzene / Irradiation

With tetrabutylammomium bromide; In water; chlorobenzene; benzene;

DOI:10.1016/S0040-4039(02)01476-4

Reference yield:

7,22-bis(benzyloxy)-3-oxahexacyclo[7.6.6.25,8.01,5.010,15.016,21]tricosa-6,10,12,14,16,18,20,22-octaene (496839-79-3) → C22H18O3 + C29H24O3

Guidance literature:

With formic acid;

DOI:10.1016/S0040-4039(02)01476-4

upstream raw materials:

9-{[3,5-bis(benzyloxy)benzyloxy]methyl}anthracene

3,5-dibenzyloxybenzyl alcohol

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