C₂₅H₂₈N₄O₃

Base Information

Chemical Name:C₂₅H₂₈N₄O₃
CAS No.:1369586-24-2
Molecular Formula:C₂₅H₂₈N₄O₃
Molecular Weight:432.522
Hs Code.:

C<sub>25</sub>H<sub>28</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₂₅H₂₈N₄O₃

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Chemical Property of C₂₅H₂₈N₄O₃

Chemical Property:

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Technology Process of C₂₅H₂₈N₄O₃

There total 7 articles about C₂₅H₂₈N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369586-20-8
(E)-1-(6-{3-[1-(6-bromo-pyridin-2-yl)-eth-(E)-ylideneaminooxy]-propyl}-pyridin-2-yl)-ethanone O-methyl-oxime

: 5720-06-9
2-Methoxyphenylboronic acid

: 1369586-24-2
C₂₅H₂₈N₄O₃

Guidance literature:: With potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; In toluene; at 100 ℃; for 16h; Inert atmosphere;

Reference yield:

: 49669-13-8
1-(6-bromopyridin-2-yl)-ethanone

: 1369586-24-2
C₂₅H₂₈N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; sodium acetate / methanol / 24 h / 20 °C

2.1: sodium hexamethyldisilazane / N,N-dimethyl-formamide; acetonitrile; tetrahydrofuran / 0.33 h / 0 - 20 °C

2.2: 16 h / 20 °C

3.1: hydrogen / platinum (IV) oxide hydrate / ethanol / 0.5 h

4.1: potassium phosphate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene / 16 h / 100 °C / Inert atmosphere

With potassium phosphate; hydroxylamine hydrochloride; hydrogen; sodium acetate; sodium hexamethyldisilazane; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; platinum (IV) oxide hydrate; palladium diacetate; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 1369588-24-8
1-[6-(3-hydroxy-prop-1-yn-1-yl)-pyridin-2-yl]-ethanone

: 1369586-24-2
C₂₅H₂₈N₄O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium acetate / methanol / 16 h / 20 °C

2.1: triethylamine / dichloromethane / 1.67 h / 0 - 20 °C

3.1: sodium hexamethyldisilazane / N,N-dimethyl-formamide; acetonitrile; tetrahydrofuran / 0.33 h / 0 - 20 °C

3.2: 16 h / 20 °C

4.1: hydrogen / platinum (IV) oxide hydrate / ethanol / 0.5 h

5.1: potassium phosphate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene / 16 h / 100 °C / Inert atmosphere

With potassium phosphate; hydrogen; sodium acetate; sodium hexamethyldisilazane; triethylamine; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; platinum (IV) oxide hydrate; palladium diacetate; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;