4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide

Base Information

• Chemical Name: 4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide
• CAS No.: 199275-42-8
• Molecular Formula: C₁₂H₁₃N₅OS₃
• Molecular Weight: 339.466

Synonyms:4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide

Chemical Property of 4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide

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Technology Process of 4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide

There total 1 articles about 4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

phenyl isothiocyanate (103-72-0) + 5-methyl-1,3,4-thiadiazol-2-ylthioacetic acid hydrazide (178316-82-0) → 4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide (199275-42-8)

Guidance literature:

In ethanol; for 0.0166667h; Irradiation;

Reference yield: 88.0%

4-Nitrophenacyl bromide (99-81-0) + 4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide (199275-42-8) → N'-[(4-nitrophenyl-3-phenylthiazol-2(3H)-ylidene)]-2-[(5-methyl-1,3,4-thiadiazol-2-yl)thio]acetohydrazide (1574548-90-5)

Guidance literature:

In ethanol; for 5h; Reflux;

DOI:10.1016/j.ejmech.2013.12.060

Reference yield: 86.0%

para-bromophenacyl bromide (99-73-0,132309-76-3) + 4-phenyl-1-[(5-methyl-1,3,4-thiadiazol-2-ylsulfanyl)acetyl]thiosemicarbazide (199275-42-8) → N'-[(4-bromophenyl-3-phenylthiazol-2(3H)-ylidene)]-2-[(5-methyl-1,3,4-thiadiazol-2-yl)thio]acetohydrazide (1574548-95-0)

Guidance literature:

In ethanol; for 5h; Reflux;

DOI:10.1016/j.ejmech.2013.12.060

upstream raw materials:

phenyl isothiocyanate

5-methyl-1,3,4-thiadiazol-2-ylthioacetic acid hydrazide

Downstream raw materials:

N'-[(4-nitrophenyl-3-phenylthiazol-2(3H)-ylidene)]-2-[(5-methyl-1,3,4-thiadiazol-2-yl)thio]acetohydrazide

N'-[(4-methylphenyl-3-phenylthiazol-2(3H)-ylidene)]-2-[(5-methyl-1,3,4-thiadiazol-2-yl)thio]acetohydrazide

N'-[(4-methoxyphenyl-3-phenylthiazol-2(3H)-ylidene)]-2-[(5-methyl-1,3,4-thiadiazol-2-yl)thio]acetohydrazide

N'-[(4-fluorophenyl-3-phenylthiazol-2(3H)-ylidene)]-2-[(5-methyl-1,3,4-thiadiazol-2-yl)thio]acetohydrazide

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