(S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one

Base Information

Chemical Name:(S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one
CAS No.:1191954-34-3
Molecular Formula:C₃₂H₃₆N₂O₂
Molecular Weight:480.65
Hs Code.:

Synonyms:(S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one

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Chemical Property of (S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one

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Technology Process of (S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one

There total 3 articles about (S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₃₈N₂O₃

: 1191954-34-3
(S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one

Guidance literature:: C₃₂H₃₈N₂O₃; With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; for 72h; Reflux; Inert atmosphere;

With acetic acid; at 20 ℃; for 0.5h;
DOI:10.1002/adsc.200800789

Reference yield:

: C₃₂H₃₈N₂O₃

: 1191954-34-3
(S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; Inert atmosphere; Reflux;
DOI:10.3762/bjoc.7.108

Reference yield:

: 630-18-2
tert-butyl isocyanide

: 95437-43-7
(S)-2-(N,N-dibenzylamino)-3-phenylpropanoic acid

: 1191954-34-3
(S)-2-tert-butyl-6-(1-dibenzylamino-2-phenylethyl)-3-methoxypyridin-4(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / -40 °C / Inert atmosphere

1.2: Inert atmosphere; Cooling

1.3: 20 °C / Inert atmosphere; Cooling

2.1: trimethylsilyl trifluoromethanesulfonate; triethylamine / dichloromethane / Inert atmosphere; Reflux

With n-butyllithium; trimethylsilyl trifluoromethanesulfonate; triethylamine; In diethyl ether; hexane; dichloromethane;
DOI:10.3762/bjoc.7.108