methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside
CAS No.:126412-70-2
Molecular Formula:C₃₃H₄₂O₆Si
Molecular Weight:562.778
Hs Code.:

Synonyms:methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside

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Technology Process of methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside

There total 3 articles about methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 107735-20-6
[(dimethylphenylsilyl)methyl]magnesium chloride

: 126412-69-9
methyl 3-O-allyl-2,4-di-O-benzyl-α-D-manno-hexodialdo-1,5-pyranoside

: 126412-70-2
methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1002/recl.19921110306

Reference yield:

: 107735-20-6
[(dimethylphenylsilyl)methyl]magnesium chloride

: 126412-69-9
methyl 3-O-allyl-2,4-di-O-benzyl-α-D-manno-hexodialdo-1,5-pyranoside

: 126412-70-2
methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside

: 126412-70-2
(S)-1-((2R,3S,4S,5S,6S)-4-Allyloxy-3,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-2-(dimethyl-phenyl-silanyl)-ethanol

Guidance literature:: In various solvent(s); at 0 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/0008-6215(89)85198-5

Reference yield:

: 107735-20-6
[(dimethylphenylsilyl)methyl]magnesium chloride

: 126412-69-9
methyl 3-O-allyl-2,4-di-O-benzyl-α-D-manno-hexodialdo-1,5-pyranoside

: 126412-70-2
methyl 3-O-allyl-2,4-di-O-benzyl-7-(phenyldimethylsilyl)-7-deoxy-L-glycero-α-D-manno-heptopyranoside

: 126412-70-2
(S)-1-((2R,3S,4S,5S,6S)-4-Allyloxy-3,5-bis-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-2-(dimethyl-phenyl-silanyl)-ethanol

Guidance literature:: In various solvent(s); at 0 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/0008-6215(89)85198-5