(E)-2-iodo-2-(4-phenyl-2-(p-tolyl)oxazol-5(4H)-ylidene)ethyl 4-methylbenzoate

Base Information

• Chemical Name: (E)-2-iodo-2-(4-phenyl-2-(p-tolyl)oxazol-5(4H)-ylidene)ethyl 4-methylbenzoate
• CAS No.: 1582306-60-2
• Molecular Formula: C₂₆H₂₂INO₃
• Molecular Weight: 523.37

Synonyms:(E)-2-iodo-2-(4-phenyl-2-(p-tolyl)oxazol-5(4H)-ylidene)ethyl 4-methylbenzoate

Chemical Property of (E)-2-iodo-2-(4-phenyl-2-(p-tolyl)oxazol-5(4H)-ylidene)ethyl 4-methylbenzoate

Chemical Property:

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Technology Process of (E)-2-iodo-2-(4-phenyl-2-(p-tolyl)oxazol-5(4H)-ylidene)ethyl 4-methylbenzoate

There total 1 articles about (E)-2-iodo-2-(4-phenyl-2-(p-tolyl)oxazol-5(4H)-ylidene)ethyl 4-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-(4-methyl-N-tosylbenzamido)-4-phenylbut-2-yn-1-yl 4-methylbenzoate (1448228-13-4) → (E)-2-iodo-2-(4-phenyl-2-(p-tolyl)oxazol-5(4H)-ylidene)ethyl 4-methylbenzoate (1582306-60-2)

Guidance literature:

With N-iodo-succinimide; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1021/jo5001719

Reference yield: 80.0%

(E)-2-iodo-2-(4-phenyl-2-(p-tolyl)oxazol-5(4H)-ylidene)ethyl 4-methylbenzoate (1582306-60-2) → 2-oxo-2-(4-phenyl-2-(p-tolyl)oxazol-5-yl)ethyl 4-methylbenzoate (1582306-75-9)

Guidance literature:

With oxygen; In 1,2-dichloro-ethane; at 80 ℃;

DOI:10.1021/jo5001719

upstream raw materials:

4-(4-methyl-N-tosylbenzamido)-4-phenylbut-2-yn-1-yl 4-methylbenzoate

Downstream raw materials:

2-oxo-2-(4-phenyl-2-(p-tolyl)oxazol-5-yl)ethyl 4-methylbenzoate

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