4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside

Base Information

Chemical Name:4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside
CAS No.:1315205-66-3
Molecular Formula:C₇₄H₈₂O₁₇S
Molecular Weight:1275.52
Hs Code.:

4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside

Synonyms:4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside

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Chemical Property of 4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside

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Technology Process of 4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside

There total 1 articles about 4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 2746-25-0
p-Methoxybenzyl bromide

: 27894-87-7
phenyl β-D-glucopyranosyl-(1->4)-1-thio-β-D-glucopyranoside

: 1315205-66-3
4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside

Guidance literature:: phenyl β-D-glucopyranosyl-(1->4)-1-thio-β-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

p-Methoxybenzyl bromide; In N,N-dimethyl-formamide; toluene; at 0 - 20 ℃; for 0.833333h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.04.048

Reference yield: 99.0%

: 1315205-66-3
4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside

: 1315205-68-5
4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol

Guidance literature:: 4-O-[2',3',4',6'-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucopyranose β-phenylthioglycoside; With N-Bromosuccinimide; In water; acetone; at 0 ℃; for 0.0833333h; Inert atmosphere;

With sodium tetrahydroborate; In ethanol; dichloromethane; at 20 ℃; for 12.5h; Inert atmosphere; Cooling with ice;

With hydrogenchloride; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmc.2011.04.048