N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine

Base Information

Chemical Name:N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine
CAS No.:102226-76-6
Molecular Formula:C₂₅H₃₅N₃O₅
Molecular Weight:457.57
Hs Code.:

Synonyms:N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine

Chemical Property:

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Technology Process of N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine

There total 5 articles about N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102226-75-5
N-(3,4-dimethoxy-phenyl)-ethylenediamine

: 85175-65-1
7,8-dimethoxy-3-(3-chloropropyl)-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one

: 102226-76-6
N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine

Guidance literature:

Reference yield:

: 73942-87-7
7,8-Dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one

: 102226-76-6
N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / dimethyl sulfoxide; acetone

2: palladium/charcoal; water; acetic acid

With potassium tert-butylate; In palladium/charcoal; water; acetic acid; dimethyl sulfoxide; acetone;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 102226-76-6
N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(3,4-dimethoxyphenylamino)-ethylamine

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / dichloromethane

2: triethylamine / dichloromethane

3: hydrogenchloride; acetic acid

4: potassium tert-butylate / dimethyl sulfoxide; acetone

5: palladium/charcoal; water; acetic acid

With thionyl chloride; potassium tert-butylate; triethylamine; In hydrogenchloride; palladium/charcoal; dichloromethane; water; acetic acid; dimethyl sulfoxide; acetone;