C₅₀H₄₉ClO₅

Base Information

Chemical Name:C₅₀H₄₉ClO₅
CAS No.:1413373-23-5
Molecular Formula:C₅₀H₄₉ClO₅
Molecular Weight:765.389
Hs Code.:

C<sub>50</sub>H<sub>49</sub>ClO<sub>5</sub>

Synonyms:C₅₀H₄₉ClO₅

Suppliers and Price of C₅₀H₄₉ClO₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₀H₄₉ClO₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₀H₄₉ClO₅

There total 10 articles about C₅₀H₄₉ClO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1413373-21-3
C₅₀H₄₉ClO₆

: 1413373-23-5
C₅₀H₄₉ClO₅

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -20 ℃; for 2.5h; Inert atmosphere;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1413373-23-5
C₅₀H₄₉ClO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: magnesium / ethylene dibromide / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

5.2: 3 h / 25 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2.5 h / -20 °C / Inert atmosphere

With pyridine; triethylsilane; oxalyl dichloride; boron trifluoride diethyl etherate; magnesium; dimethyl sulfoxide; L-proline; trichlorophosphate; ethylene dibromide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 1413373-23-5
C₅₀H₄₉ClO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: magnesium / ethylene dibromide / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

5.2: 3 h / 25 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2.5 h / -20 °C / Inert atmosphere

With triethylsilane; sodium tetrahydroborate; n-butyllithium; boron trifluoride diethyl etherate; potassium carbonate; magnesium; dimethyl sulfoxide; trifluoroacetic anhydride; 18-crown-6 ether; ethylene dibromide; In tetrahydrofuran; hexane; dichloromethane; toluene;